Patent · US Expired

Method for disentangling hollow carbon microfibers, electrically conductive transparent carbon microfibers aggregation film amd coating for forming such film

US5853877A · kind A · utility

109Cited by
9References
20Claims
0Family size

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Key dates

Filing dateMay 31, 1996
Grant dateDec 29, 1998
Priority date
Expiry dateMay 31, 2016

Classification

  • Technology area (CPC Y)Emerging Cross-Sectional Technologies
  • CPC primaryY10T428/2933
  • WIPO fieldMicro-structural and nano-technology
  • WIPO sectorChemistry

Abstract

This invention relates to a method for disentangling hollow carbon microfibers and to the dispersion of hollow carbon microfibers, preferably having an outer diameter of 3.5 to 70 nm and an aspect ratio of at least 5, to form transparent electrically conductive films. Hollow carbon microfibers, treated with strong acids such as sulfuric acid or oleum and an oxidizing agent such as nitric acid, are disentangled and dispersed homogeneously in a polar solvent. The slurry in which the microfibers are suspended can be coated on a substrate. The coating film is dried and a transparent electrically conductive film is formed. A carbon microfiber aggregation film with excellent transparency is obtained having a total transmittance of at least 80 percent and a haze value of at most 0.1%.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.