Preparation process of supported catalyst for the synthesis of methacrolein and methacrylic acid
US5856259A · kind A · utility
Assignee
Inventors
Key dates
| Filing date | Jun 20, 1997 |
| Grant date | Jan 5, 1999 |
| Priority date | — |
| Expiry date | Jun 20, 2017 |
Classification
- Technology area (CPC B)Performing Operations; Transporting
- CPC primaryB01J2523/00
- WIPO fieldOrganic fine chemistry
- WIPO sectorChemistry
Abstract
A process for producing a supported catalyst for the synthesis of methacrolein and methacrylic acid in which a catalytic active substance comprising a composite oxide containing molybdenum and bismuth as essential components is supported on the inside surface and/or the outside surface of an inert carrier, which comprises the steps of drying a mixed solution or an aqueous slurry containing the compounds of the elements constituting the catalytic active substance, subjecting the dried product to a primary calcination at a temperature in a range of 200.degree.-400.degree. C. to form a catalytic active substance precursor, comminuting the obtained catalytic active substance precursor to such an extent that the medium particle size in the volume-based particle size distribution becomes 10 .mu.m or less, supporting the comminution product on an inert carrier, and subjecting it to a secondary calcination at a temperature which is 100.degree. C. or more higher than the primary calcination temperature.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.