Method of forming particles using a supercritical fluid
US5864923A · kind A · utility
Assignees
Inventors
Key dates
| Filing date | Aug 26, 1997 |
| Grant date | Feb 2, 1999 |
| Priority date | — |
| Expiry date | Aug 26, 2017 |
Classification
- Technology area (CPC B)Performing Operations; Transporting
- CPC primaryB01J13/0091
- WIPO fieldPharmaceuticals
- WIPO sectorChemistry
Abstract
A method for providing aerogels, and aerogels produced according to the method, is described. As one aspect, antiperspirant compounds that are in aerogel form, and antiperspirant and deodorant compositions including such salts, are described. The method involves contacting a solution containing material to be processed with a species selected to precipitate the material and selected so as to be miscible with the solvent system of the solution. After the material is precipitated, the material may be washed with the precipitating species until it is substantially free of solvent system. Then, the precipitating species containing the material precipitate is taken above its critical point, and the supercritical fluid is exhausted above its critical temperature. Alternately, a separate isolating species is introduced to displace the precipitating species, or the precipitating species/solvent system mixture. The isolating species then is taken above its critical point, and exhausted above its critical temperature. The invention provides for batch or continuous processes.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.