Patent · US Expired

Flow tube for NMR probe

US5867026A · kind A · utility

15Cited by
7References
46Claims
0Family size

Assignee

Inventor

Key dates

Filing dateApr 4, 1996
Grant dateFeb 2, 1999
Priority date
Expiry dateApr 4, 2016

Classification

  • Technology area (CPC G)Physics
  • CPC primaryG01R33/307
  • WIPO fieldMeasurement
  • WIPO sectorInstruments

Abstract

A three-piece NMR detection cell comprises an inlet tube having a conically, tapered outlet nozzle, leading to an analysis tube, in turn leading to an outlet tube having a conically tapered inlet nozzle. The inlet and outlet tubes are inserted into the analysis tube at a distance from their inserted ends and sealed in a manner appropriate to their composition. When the detection cell is used in a coupled HPLC-NMR apparatus, increased NMR sensitivity and improved lineshape are obtained at low injection volumes while maintaining a low level of chromatographic band broadening and a high level of magnetic field homogeneity.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.