Patent · US Expired

Resolution

US5892093A · kind A · utility

1Cited by
0References
3Claims
0Family size

Assignee

Inventors

Key dates

Filing dateFeb 7, 1997
Grant dateApr 6, 1999
Priority date
Expiry dateFeb 7, 2017

Classification

  • Technology area (CPC C)Chemistry; Metallurgy
  • CPC primaryC07B2200/07
  • WIPO fieldOrganic fine chemistry
  • WIPO sectorChemistry

Abstract

A reproducible process for preparing a substantially single enantiomer (R or S) of 4-cyano-4-(3,4-dimethoxyphenyl)-5-methylhexanoic acid, or an analogue thereof, thereby providing single enantiomer acid for the first time, proceeds by means of a classical salt resolution employing a resolving agent selected from an enantiomer (R or S) of a 1-arylalkylamine and (-)-quinine, and provides novel salts that are readily convertible to verapamil.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.