Patent · US Expired

Multiwall polymeric microspheres

US5912017A · kind A · utility

60Cited by
14References
5Claims
0Family size

Assignee

Inventors

Key dates

Filing dateJul 1, 1992
Grant dateJun 15, 1999
Priority date
Expiry dateJul 1, 2012

Classification

  • Technology area (CPC Y)Emerging Cross-Sectional Technologies
  • CPC primaryY10T428/2989
  • WIPO fieldPharmaceuticals
  • WIPO sectorChemistry

Abstract

A method for preparation of multi-layer polymeric microspheres formed from any degradable or non-degradable polymers which are not soluble in each other at a particular concentration, but which have a positive spreading coefficient in solution. The multi-layer microspheres produced by the method are distinguished by extremely uniform dimensioned layers of polymer and actual incorporation of the substance to be delivered into the polymer layers. In the preferred embodiment of the method, two polymers are dissolved in a volatile organic solvent, the substance to be incorporated is dispersed or dissolved in the polymer solution, the mixture is suspended in an aqueous solution and stirred, and the solvent is slowly evaporated, creating microspheres with an inner core formed by one polymer and an outer layer formed by the second polymer. In another embodiment, solvent is removed by spray drying. In still another embodiment, polymers are melted and combined with the substance to be incorporated, then cooled to form layered microspheres.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.