Recovery of catalyst systems from diaryl carbonate-containing reaction solutions by suspension crystallization
US5965472A · kind A · utility
Assignee
Inventors
Key dates
| Filing date | Apr 1, 1997 |
| Grant date | Oct 12, 1999 |
| Priority date | — |
| Expiry date | Apr 1, 2017 |
Classification
- Technology area (CPC C)Chemistry; Metallurgy
- CPC primaryC07C68/01
- WIPO fieldOrganic fine chemistry
- WIPO sectorChemistry
Abstract
Catalyst systems with a content of a platinum-group-metal catalyst, a co-catalyst, a quaternary salt and a base for the oxidative carbonylation of aromatic hydroxy compounds to the corresponding diaryl carbonates are according to the invention obtained as a mother liquor by suspension crystallization and can be returned into the carbonylation reaction or worked up to valuable materials. The crystallizate, which consists predominantly of diaryl carbonate and the parent aromatic hydroxy compound, is worked up to pure diaryl carbonate and pure hydroxy compound.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.