Patent · US Expired

Polyvinyl alcohol compositions prepared by crosslinking in a freezing step

US5972375A · kind A · utility

97Cited by
4References
14Claims
0Family size

Assignee

Inventors

Key dates

Filing dateDec 23, 1997
Grant dateOct 26, 1999
Priority date
Expiry dateDec 23, 2017

Classification

  • Technology area (CPC C)Chemistry; Metallurgy
  • CPC primaryC08L35/08
  • WIPO fieldMacromolecular chemistry, polymers
  • WIPO sectorChemistry

Abstract

The invention provides a translucent, water-insoluble hydrogel composition and methods of making it. The hydrogel composition comprises a polyvinyl alcohol polymer and a complexing agent which are physically crosslinked to form a semi-crystalline polyvinyl alcohol-complexing agent polymer complex. This is achieved by: PA1 (i) combining a polyvinyl alcohol polymer with a suitable aprotic solvent; PA1 (ii) Adding a complexing agent to (i) to form a water soluble complex with the polyvinyl alcohol polymer; and PA1 (iii) Allowing the polyvinyl alcohol polymer and the complexing agent to form a water-insoluble, semi-crystalline structure. The formation of the semi-crystalline structure is assisted by freezing the polyvinyl alcohol/complexing agent/polar aprotic solvent mixture.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.