Patent · US Expired

Composite polyamide reverse osmosis membrane and method of producing the same

US6015495A · kind A · utility

37Cited by
13References
61Claims
0Family size

Assignee

Inventors

Key dates

Filing dateFeb 18, 1998
Grant dateJan 18, 2000
Priority date
Expiry dateFeb 18, 2018

Classification

  • Technology area (CPC B)Performing Operations; Transporting
  • CPC primaryB01D71/56
  • WIPO fieldChemical engineering
  • WIPO sectorChemistry

Abstract

A composite polyamide reverse osmosis membrane and method of producing same. In a preferred embodiment, the membrane is made by coating a porous polysulfone support for about 1 minute with an aqueous solution containing 2 wt % m-phenylenediamine (MPD), 2 wt % 2-butoxyethanol and 2 wt % propylene glycol. Next, the excess MPD solution is removed, and the coated support is dipped for about 1 minute in 0.1 wt % organic solvent solution of trimesoyl chloride (TMC) in a mixture of alkanes having from 8 to 12 carbon atoms. After draining the TMC solution off, the resulting composite membrane is air dried at room temperature to 40.degree. C. for about 1 minute and then rinsed in a basic aqueous solution at 40-60.degree. C. for 1 to 30 minutes. The resultant membrane exhibits a flux of 27.5 gfd and a salt rejection of 98.2% when used at 225 psi for an aqueous solution containing 2000 ppm of NaCl.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.