Patent · US Expired

Oxidation process using tempo

US6031101A · kind A · utility

7Cited by
0References
15Claims
0Family size

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Inventors

Key dates

Filing dateApr 1, 1999
Grant dateFeb 29, 2000
Priority date
Expiry dateApr 1, 2019

Classification

  • Technology area (CPC C)Chemistry; Metallurgy
  • CPC primaryC07D405/04
  • WIPO fieldOrganic fine chemistry
  • WIPO sectorChemistry

Abstract

The present invention relates to an oxidation using sodium chlorite in the presence of a catalytic amount of TEMPO and sodium hypochlorite which converts the penultimate intermediate bearing a primary alcohol to the target endothelin antagonist compound of Formula I having a carboxylic acid ##STR1##

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.