Methods of PHA extraction and recovery using non-halogenated solvents
US6043063A · kind A · utility
Assignee
Inventors
Key dates
| Filing date | Apr 14, 1998 |
| Grant date | Mar 28, 2000 |
| Priority date | — |
| Expiry date | Apr 14, 2018 |
Classification
- Technology area (CPC Y)Emerging Cross-Sectional Technologies
- CPC primaryY02W30/62
- WIPO fieldMacromolecular chemistry, polymers
- WIPO sectorChemistry
Abstract
Polyhydroxyalkanoate (PHA) polyester is extracted from biomass by dissolving the PHA in a non-halogenated solvent which comprises a PHA-good solvent or a mixture thereof. Suitable PHA-good solvents can be selected from the disclosed alcohols, esters, amides and ketones. The PHA can be recovered, for example, by cooling, by solvent evaporation, or by addition of a PHA-poor solvent, wherein the PHA-poor solvent preferably dissolves less than about 1% (w/v) of the PHA at a temperature below the solvent boiling point. Preferred PHA types for use in the invention are poly (hydroxybutyrate-co-hydroxyvalerate), poly(3-hydroxybutyrate-co-4-hydroxybutyrate), and polymers/copolymers of hydroxyterminated polyhydroxybutyrate.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.