Method for making lithiated metal oxide
US6083475A · kind A · utility
Assignee
Inventors
Key dates
| Filing date | Apr 2, 1999 |
| Grant date | Jul 4, 2000 |
| Priority date | — |
| Expiry date | Apr 2, 2019 |
Classification
- Technology area (CPC Y)Emerging Cross-Sectional Technologies
- CPC primaryY02E60/10
- WIPO fieldElectrical machinery, apparatus, energy
- WIPO sectorElectrical engineering
Abstract
The present invention is a simple and reliable method for producing lithiated metal oxides such as those useful as cathode materials in lithium ion electrochemical cells. The method is based on the use of an organic solvent that dissolves both lithium sulfide and elemental sulfur without dissolving the metal oxide or the lithiated product. Lithium sulfide and the metal oxide as a powder are refluxed in the organic solvent under an inert atmosphere. The organic solvent dissolves the lithium sulfide and the dissolved sulfide reduces the metal oxide allowing the intercalation of lithium. At the same time the sulfur that results from the oxidation-reduction reaction is carried away by the solvent thereby promoting the reaction and preventing contamination of the product with sulfur.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.