Patent · US Expired

Surface-modified cellulose microfibrils, method for making the same, and use thereof as a filler in composite materials

US6117545A · kind A · utility

93Cited by
0References
27Claims
0Family size

Assignee

Inventors

Key dates

Filing dateJul 9, 1998
Grant dateSep 12, 2000
Priority date
Expiry dateJul 9, 2018

Classification

  • Technology area (CPC Y)Emerging Cross-Sectional Technologies
  • CPC primaryY10T428/2978
  • WIPO fieldMacromolecular chemistry, polymers
  • WIPO sectorChemistry

Abstract

Cellulose microfibrils, in particular for use as a reinforcing filler or structuring agent in composite materials, a method for making same, and composite materials containing said microfibrils, are disclosed. Specifically, said microfibrils are surface-modified cellulose microfibrils with an L/D ratio higher than 20, preferably higher than 100, and an average diameter of 1-50 nm, where L is the length of the microfibril and D is its average diameter. At least 25% by number of the hydroxyl functions on the surface of the microfibrils are esterified by at least one organic compound including at least one function capable of reacting with the hydroxyl groups of the cellulose. As a result, when the organic compound is a compound that includes acetyl groups such as acetic acid, said microfibrils are used as a reinforcing filler in a material comprising cellulose acetate as the polymeric matrix. The filled composite material may be shaped to provide films, moldings, fibers or yarns.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.