Patent · US Expired

Method for production of cross-linked polymer

US6194531A · kind A · utility

21Cited by
11References
18Claims
0Family size

Assignee

Inventors

Key dates

Filing dateJun 3, 1997
Grant dateFeb 27, 2001
Priority date
Expiry dateJun 3, 2017

Classification

  • Technology area (CPC C)Chemistry; Metallurgy
  • CPC primaryC08F2/10
  • WIPO fieldMacromolecular chemistry, polymers
  • WIPO sectorChemistry

Abstract

A method for producing a cross-linked polymer manifesting a high absorption capacity and having a small content of soluble component by a convenient and expeditious process with high productivity is provided. An absorbent resin such that disposable diapers and other products incorporating the absorbent resin manifest outstanding qualities and a method for the production of the absorbent resin are proposed. The cross-linked polymer according to this invention is produced by a method of polymerizing an aqueous polymerizable monomer solution containing a water-soluble ethylenically unsaturated monomer and a first cross-linking agent capable of forming a hydrogel polymer by polymerization, which method comprises the steps of performing the polymerization in a substantially static state from the time at which the polymerization is initiated till the time at which the whole polymerization system is gelated, subsequently giving the polymerization system a thorough shearing force thereby granulating the hydrogel polymer before the polymerization system has the temperature thereof elevated by the heat of polymerization to the highest level, and further continuing the polymerization.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.