Patent · US Expired

Methods for high throughout determination and ranking of formulations and solubility

US6271038A · kind A · utility

15Cited by
22References
17Claims
0Family size

Assignee

Inventors

Key dates

Filing dateDec 15, 1999
Grant dateAug 7, 2001
Priority date
Expiry dateDec 15, 2019

Classification

  • Technology area (CPC Y)Emerging Cross-Sectional Technologies
  • CPC primaryY10T436/2575
  • WIPO fieldMeasurement
  • WIPO sectorInstruments

Abstract

The invention provides apparatus and methods for formulation mixing and measurement to produce rank orders of solubility of chemicals in a variety of formulations. One such method includes mixing a volume of a stock solution having a known concentration of a chemical with a volume of a base liquid to form a control sample. Another volume of the stock solution is mixed with a volume of a formulation to form a test sample. The control sample is passed through a capillary electrochromatography (CEC) tube to separate the chemical from the base liquid, and the test sample is passed through a CEC tube to separate the chemical from the formulation. The method includes measuring the amount of chemical passing through the CEC tubes for both the control sample and the test sample, and comparing the measured amount of chemical from the control sample with the measured amount of chemical from the test sample to determine the solubility of the chemical in the formulation relative to the base liquid.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.