Process for preparing 1,3-diketones
US6310258A · kind A · utility
Assignee
Inventors
Key dates
| Filing date | Jul 31, 2000 |
| Grant date | Oct 30, 2001 |
| Priority date | — |
| Expiry date | Jul 31, 2020 |
Classification
- Technology area (CPC B)Performing Operations; Transporting
- CPC primaryB01J2219/00155
- WIPO fieldChemical engineering
- WIPO sectorChemistry
Abstract
The invention provides a process for preparing 1,3-diketones by rearrangement of the isomeric enol ester in a tube reactor comprising a heated portion and an unheated insulated portion which can optionally be provided with cooling means. The unheated portion of the reactor has a higher volume to surface ratio than the heated portion of the reactor. The reaction can be carried out adiabatically in the unheated portion of the reactor. The process and apparatus provide higher yields and selectivity to the 1,3-diketones.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.