Patent · US Expired

Dewatering and purification of crude pyrrolidine

US6353118B1 · kind B1 · utility

0Cited by
2References
6Claims
0Family size

Assignee

Inventors

Key dates

Filing dateNov 20, 2000
Grant dateMar 5, 2002
Priority date
Expiry dateNov 20, 2020

Classification

  • Technology area (CPC C)Chemistry; Metallurgy
  • CPC primaryC07D295/023
  • WIPO fieldOrganic fine chemistry
  • WIPO sectorChemistry

Abstract

In a process for purifying crude pyrrolidine to give a pyrrolidine composition comprising more than 99% (m/m) of pyrrolidine and less than 0.3% (m/m) of water, crude pyrrolidine comprising from 40 to 98% (m/m) of pyrrolidine and having a water content of more than 2% (m/m) is subjected to continuous distillation at a pressure at the top of less than 950 hPa in a column having a stripping section and a rectifying section.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.