Dewatering and purification of crude pyrrolidine
US6353118B1 · kind B1 · utility
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2References
6Claims
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Key dates
| Filing date | Nov 20, 2000 |
| Grant date | Mar 5, 2002 |
| Priority date | — |
| Expiry date | Nov 20, 2020 |
Classification
- Technology area (CPC C)Chemistry; Metallurgy
- CPC primaryC07D295/023
- WIPO fieldOrganic fine chemistry
- WIPO sectorChemistry
Abstract
In a process for purifying crude pyrrolidine to give a pyrrolidine composition comprising more than 99% (m/m) of pyrrolidine and less than 0.3% (m/m) of water, crude pyrrolidine comprising from 40 to 98% (m/m) of pyrrolidine and having a water content of more than 2% (m/m) is subjected to continuous distillation at a pressure at the top of less than 950 hPa in a column having a stripping section and a rectifying section.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.