Patent · US Expired

Post conversion of a gas containing hydrogen sulphide, the elimination of sulphur crystallized by cooling

US6413488B1 · kind B1 · utility

4Cited by
5References
20Claims
0Family size

Assignee

Inventors

Key dates

Filing dateJun 19, 2000
Grant dateJul 2, 2002
Priority date
Expiry dateJun 19, 2020

Classification

  • Technology area (CPC C)Chemistry; Metallurgy
  • CPC primaryC01B17/05
  • WIPO fieldChemical engineering
  • WIPO sectorChemistry

Abstract

A process and an apparatus are described for treatment of a gas containing hydrogen sulphide and sulphur dioxide, for example a Claus plant tail gas, in which the gas is brought into contact with an organic solvent (1) e.g. polyethylene glycol 400, containing a catalyst e.g. sodium salicylate, in at least one gas-liquid reactor-contactor (2) and a gas (20) substantially no longer containing hydrogen sulphide and sulphur dioxide is recovered. A single-phase solution (4) of solvent and sulphur is extracted from the reactor-contactor and a portion is cooled in at least one cooling zone (8) to obtain a suspension of sulphur crystals in the solvent, the crystallised sulphur is separated from the solvent in a separation zone (10), the sulphur-depleted solvent (14, 15) is recovered and recycled at least in part to the reactor-contactor (2), and the sulphur (13) is recovered.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.