Patent · US Expired

Processing aqueous titanium chloride solutions to ultrafine titanium dioxide

US6440383B1 · kind B1 · utility

48Cited by
77References
34Claims
0Family size

Assignee

Inventors

Key dates

Filing dateFeb 14, 2000
Grant dateAug 27, 2002
Priority date
Expiry dateFeb 14, 2020

Classification

  • Technology area (CPC C)Chemistry; Metallurgy
  • CPC primaryC01P2006/12
  • WIPO fieldMaterials, metallurgy
  • WIPO sectorChemistry

Abstract

A hydrometallurgical process is provided for producing ultrafine or nano-sized titanium dioxide from titanium containing solutions, particularly titanium chloride solutions. The process is conducted by total evaporation of the solution, above the boiling point of the solution and below the temperature where there is significant crystal growth. Chemical control additives may be added to control particle size. Nano-sized elemental particles are formed after calcination. The titanium dioxide can be either anatase or rutile. Following calcination, the titanium dioxide is milled to liberate the elemental particles and provide a high quality nano-sized TiO2 with a narrow particle size distribution.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.