Patent · US Expired

Methods for the preparation and characterization of multi-substituted fullerenes

US6448412B1 · kind B1 · utility

55Cited by
5References
9Claims
0Family size

Assignee

Inventors

Key dates

Filing dateOct 30, 2000
Grant dateSep 10, 2002
Priority date
Expiry dateOct 30, 2020

Classification

  • Technology area (CPC Y)Emerging Cross-Sectional Technologies
  • CPC primaryY10S977/881
  • WIPO fieldOrganic fine chemistry
  • WIPO sectorChemistry

Abstract

The invention is directed to multiply-substituted fullerene derivatives of novel configurations, and methods for their preparation and use. The methods involve the combinatorial synthesis of a library of fullerene derivatives and comprises the steps of forming a mixture of fullerene derivatives by reacting the Cn fullerene with two or more reactive precursor compounds, and removing the unreacted compounds to yield the fullerene derivatives having the desired activity. Methods for the identification and screening of a combinatorial library of fullerenes by 3He-nuclear magnetic resonance and electrospray mass spectrometry to define members with the optimal desired activity are also provided.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.