Process for preparing a silica suspension in a silicone matrix crosslinkable by polycondensation to form elastomers
US6462104B1 · kind B1 · utility
Assignee
Inventors
Key dates
| Filing date | Aug 27, 2001 |
| Grant date | Oct 8, 2002 |
| Priority date | — |
| Expiry date | Aug 27, 2021 |
Classification
- Technology area (CPC C)Chemistry; Metallurgy
- CPC primaryC08K9/06
- WIPO fieldMacromolecular chemistry, polymers
- WIPO sectorChemistry
Abstract
The invention concerns a method for preparing a silica suspension in a silicone matrix, said suspension capable of being used for producing organopolysiloxanes crosslinkable by polycondensation. The invention aims at seeking a technical compromise between the rheology of said compositions and the mechanical properties of the resulting crosslinked elastomers. As a solution, the invention discloses a method for preparing a silica suspension treated with organosilazane in a silicone material comprising a linear reactive polyorganosiloxane bearing for example at each chain end a hydroxy group. The invention is characterized in that it consists essentially in introducing the organosilozane in the preparation medium: before and/or substantially simultaneously before bringing together at least part of the silicone material and the particulate filler used, said organosilozane introduction being carried out with a fraction of organosilazane corresponding to a proportion ranging between 8% and 30% by dry weight relatively to the silica filler, and after bringing together the filler and all or part of the silicone material.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.