Patent · US Expired

Method for distilling ammonia

US6482297B1 · kind B1 · utility

4Cited by
6References
6Claims
0Family size

Assignee

Inventors

Key dates

Filing dateJun 6, 2001
Grant dateNov 19, 2002
Priority date
Expiry dateJun 6, 2021

Classification

  • Technology area (CPC Y)Emerging Cross-Sectional Technologies
  • CPC primaryY10S203/08
  • WIPO fieldChemical engineering
  • WIPO sectorChemistry

Abstract

The present invention relates to an improved process for distilling ammonia from a mixture, more particular from a mixture resulting from the reaction between aminonitrile and water (which reaction is also called cyclizing hydrolysis). The process for distilling the ammonia contained in an aqueous caprolactam solution, uses a column with a bottom temperature less than or equal to 160° C. and at an absolute pressure less than or equal to 5 bar, the ammonia distilled at the top of the column being compressed to a pressure greater than or equal to 10 bar and then condensed at a temperature of 25° C. to 60° C.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.