Method of preparing of nanometer electrocatalyst for proton exchange membrane fuel cell
US6518217B2 · kind B2 · utility
Assignee
Inventors
Key dates
| Filing date | Aug 17, 2001 |
| Grant date | Feb 11, 2003 |
| Priority date | — |
| Expiry date | Aug 17, 2021 |
Classification
- Technology area (CPC Y)Emerging Cross-Sectional Technologies
- CPC primaryY02P70/50
- WIPO fieldChemical engineering
- WIPO sectorChemistry
Abstract
The present invention relates a method for preparing nanometer electrocatalyst for proton exchange membrane fuel cells, comprising the steps of: 1) adding in water a platinum halogen compound or a mixture of a platinum halogen compound and a ruthenium halogen compound, and active carbon, the amount of noble metal in the solution is 0.5-10 g/L, and the amount of active carbon is 0.05-2 g/L; 2) adjusting the pH of the solution to 2.5-10.5 with potassium hydroxide and/or ammonium hydroxide; 3) adding dropwise a reducing agent to an amount of 2.5 to 5 times in excess of that of the noble metal in moles, and allowing the reduction reaction to proceed; 4) filtering off the liquid and washing the remains; and 6) drying the remains. The catalysts prepared by the present invention have uniform particle sizes in the range of 4±0.5 nm, and superior electrochemical properties.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.