Patent · US Expired

Hemihydrogenation method for dinitriles

US6521779B1 · kind B1 · utility

17Cited by
4References
20Claims
0Family size

Assignee

Inventors

Key dates

Filing dateSep 25, 2001
Grant dateFeb 18, 2003
Priority date
Expiry dateSep 25, 2021

Classification

  • Technology area (CPC C)Chemistry; Metallurgy
  • CPC primaryC07D223/12
  • WIPO fieldOrganic fine chemistry
  • WIPO sectorChemistry

Abstract

The invention concerns the hydrogenation in amine function of a nitrile function of a dinitrile to obtain the corresponding aminonitrile. More precisely, the invention concerns the hemihydrogenation of a dinitrile into the corresponding aminonitrile, in a liquid medium, characterized in that it consists in operating in the presence of a Raney nickel or cobalt catalyst containing copper and/or silver and/or gold and in the presence of an alkaline or alkaline-earth metal hydroxide. The hemihydrogenation of adiponitrile provides amino-6 capronitrile, compound which can be easily transformed by cyclization hydrolysis into caprolactam, the starting product for the synthesis of polyamide-6.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.