Patent · US Expired

Process for preparing phosphoric ester

US6710199B2 · kind B2 · utility

8Cited by
3References
14Claims
0Family size

Assignee

Inventors

Key dates

Filing dateMay 30, 2002
Grant dateMar 23, 2004
Priority date
Expiry dateMay 30, 2022

Classification

  • Technology area (CPC C)Chemistry; Metallurgy
  • CPC primaryC07F9/025
  • WIPO fieldOrganic fine chemistry
  • WIPO sectorChemistry

Abstract

A process for preparing a phosphoric ester having reduced odor, comprising contacting a phosphoric ester with at least one of an inert gas and steam at 100° to 160° C. in a packed tower; a process for preparing a phosphoric ester having reduced odor, comprising repeating a set of processes comprising (A) heating a phosphoric ester, and contacting the heated phosphoric ester with at least one of an inert gas and steam; and (B) cooling the phosphoric ester obtained in the step (A); a process for preparing a phosphoric ester having reduced odor, comprising adding water to a phosphoric ester, and distilling water from the phosphoric ester under reduced pressure; and a process for preparing a phosphoric ester having reduced odor, comprising reacting an organic hydroxy compound with a phosphorylation agent, while introducing an inert gas into the mixture of the organic hydroxy compound and the phosphorylation agent. The phosphoric ester is useful for, for instance, a shampoo, a cleaning agent, a facial cleansing agent, an emulsifier, and the like.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.