Control of weight during evaporation of samples
US6722214B1 · kind B1 · utility
Assignee
Inventor
Key dates
| Filing date | Jun 8, 2000 |
| Grant date | Apr 20, 2004 |
| Priority date | — |
| Expiry date | Jun 8, 2020 |
Classification
- Technology area (CPC B)Performing Operations; Transporting
- CPC primaryB04B15/02
- WIPO fieldChemical engineering
- WIPO sectorChemistry
Abstract
A method of controlling the evaporation of liquid in samples in an evaporating centrifuge, by monitoring the centrifugal force exerted on a sample holder containing a liquid sample having solid material dissolved or otherwise mixed therein. The centrifugal force is determined using a load cell, a strain gauge or, where relative movement between sample holder and rotor is permitted albeit with resilient restraint, the centrifugal force signal may be generated by a position sensing transducer. The speed of rotation is sensed by a further transducer and both force and speed signals are conveyed to a computer programmed to generate a process control signal for controlling the evaporation process therefrom. A preferred method of control involves determining the rate of change of weight with time and terminating the evaporation process when the rate of change drops to zero. Evaporation is assisted by heating the samples and the process control signals determine not only the speed of rotation, but also the heating of the samples. A weight signal can be computed from the force signal by reference to the speed signal which is proportional to the centrifugal force acting on the sample holder…
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.