Separation process
US6964728B2 · kind B2 · utility
Inventors
Key dates
| Filing date | May 16, 2002 |
| Grant date | Nov 15, 2005 |
| Priority date | — |
| Expiry date | May 16, 2022 |
Classification
- Technology area (CPC Y)Emerging Cross-Sectional Technologies
- CPC primaryY10S203/14
- WIPO fieldChemical engineering
- WIPO sectorChemistry
Abstract
Bisphenol-A-bis(neopentylglycolphosphate) products of enhanced properties and processes for preparing them are described. One of the processes includes (a) mixing and reacting neopentyl glycol and bisphenol-A-bis(dichlorophosphate) in an inert polar organic solvent which (1) if mixed by itself with an equal volume of water at 25° C., will form a separate phase, (2) the solvent by itself will dissolve at least about 10 wt % of bisphenol-A-bis(neopentylglycolphosphate) at a temperature in the range of 25 to 50° C., and optionally but preferably (3) the solvent by itself can be completely vaporized at a temperature below about 180° C.; (b) washing bisphenol-A-bis(neopentylglycolphosphate) product formed in a) while dissolved in inert organic solvent having such characteristics at least once with an aqueous alkaline washing solution; and (c) optionally but preferably, recovering bisphenol-A-bis(neopentylglycolphosphate) product from organic solvent having such characteristics. The reaction of (a) can be conducted in an inert non-polar solvent if that solvent is replaced by an inert polar organic solvent satisfying (1) and (2), and preferably (3). A solvent satisfying (1), (2), and (3) …
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.