Patent · US Expired

Methods to increase nucleotide signals by raman scattering

US6972173B2 · kind B2 · utility

48Cited by
27References
7Claims
0Family size

Assignee

Inventors

Key dates

Filing dateMar 14, 2002
Grant dateDec 6, 2005
Priority date
Expiry dateMar 14, 2022

Classification

  • Technology area (CPC C)Chemistry; Metallurgy
  • CPC primaryC12Q1/6825
  • WIPO fieldBiotechnology
  • WIPO sectorChemistry

Abstract

The methods and apparatus disclosed herein concern nucleic acid sequencing by enhanced Raman spectroscopy. In certain embodiments of the invention, nucleotides are covalently attached to Raman labels before incorporation into a nucleic acid 13. Exonuclease 15 treatment of the labeled nucleic acid 13 results in the release of labeled nucleotides 16, 130, which are detected by Raman spectroscopy. In alternative embodiments of the invention, nucleotides 16, 130 released from a nucleic acid 13 by exonuclease 15 treatment are covalently cross-linked to silver or gold nanoparticles 140 and detected by surface enhanced Raman spectroscopy (SERS), surface enhanced resonance Raman spectroscopy (SERRS) and/or coherent anti-Stokes Raman spectroscopy (CARS). Other embodiments of the invention concern apparatus 10, 100, 210 for nucleic acid sequencing.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.