Process for making caprolactam
US7060820B1 · kind B1 · utility
Assignee
Inventors
Key dates
| Filing date | Mar 18, 2005 |
| Grant date | Jun 13, 2006 |
| Priority date | — |
| Expiry date | Mar 18, 2025 |
Classification
- Technology area (CPC C)Chemistry; Metallurgy
- CPC primaryC07D201/08
- WIPO fieldOrganic fine chemistry
- WIPO sectorChemistry
Abstract
Lactams, in particular ε-caprolactam, are produced by the hydrolytic cyclization of aminonitriles, in particular 6-aminocapronitrile, in the vapor phase in a plurality of adiabatic fixed bed reaction zones arranged in succession wherein at least a portion of the heat of the exothermic reaction is removed between each of the successive reaction zones. Conducting the reaction in such a manner requires less capital for the reactor itself. It has also been found that the product exiting such a reaction system can be directly fed to a distillation unit without the need of additional cooling or storing.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.