Process for producing ammonium polythiomolybdate
US7074381B1 · kind B1 · utility
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17Claims
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Key dates
| Filing date | Jun 13, 2005 |
| Grant date | Jul 11, 2006 |
| Priority date | — |
| Expiry date | Jun 13, 2025 |
Classification
- Technology area (CPC Y)Emerging Cross-Sectional Technologies
- CPC primaryY02P20/10
- WIPO fieldBasic materials chemistry
- WIPO sectorChemistry
Abstract
A process for preparation of an ammonium polythiomolybdate or a hydrate thereof of the formula (NH4)2Mo3S13.n H2O where n is 0, 1 or 2, in which aqueous ammonium monosulfide, elemental sulfur and molybdic oxide are reacted in a sealed reactor, with hydrogen sulfide gas being fed into the reactor until the hydrogen sulfide is no longer absorbed by the reaction mixture to form a reaction product and then heating the reaction product in a sealed reactor, the concentration of ammonium monosulfide in the reaction mixture being controlled throughout the reaction such that reactor pressure does not exceed 700 kPa (100 psig).
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.