Method of making oxide particles
US7118727B2 · kind B2 · utility
Assignee
Inventor
Key dates
| Filing date | Jun 16, 2003 |
| Grant date | Oct 10, 2006 |
| Priority date | — |
| Expiry date | Oct 2, 2024 |
Classification
- Technology area (CPC Y)Emerging Cross-Sectional Technologies
- CPC primaryY10S977/811
- WIPO fieldMaterials, metallurgy
- WIPO sectorChemistry
Abstract
The present invention provides a process for producing particles, such as oxide nanoparticles, in a substantially water-free environment. The process involves mixing at least one metal compound of the formula MX(m−n) with at least one surfactant and at least one solvent, wherein M is an electropositive element of Groups 1–15; each X is independently selected from the group consisting of O1/2, F, Cl, Br, I, OR, O2CR, NR2, and R; each R is independently a hydrocarbyl group; n is equal to ½ the oxidation state of the metal M in the product particle; and m is equal to the oxidation state of the element M. The components are typically combined to form a mixture which is thermally treated for a time period sufficient to convert the metal compound into particles of the corresponding oxide, having sizes in a range between about 0.5 nanometer and about 1000 nanometers. Examples of metal compounds employed in this process include materials such as Si(OR)4, Ti(OR)4 (where R is as described above), (Zr(OiPr)2)(OAc)2, and the like. Illustrative oxide materials which can be prepared by this process include TiO2, ZrO2, SiO2, and B2O3.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.