Patent · US Expired

Hetero diels-alder adducts of pentacene as soluble precursors of pentacene

US7125989B2 · kind B2 · utility

9Cited by
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25Claims
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Key dates

Filing dateNov 20, 2002
Grant dateOct 24, 2006
Priority date
Expiry dateMar 7, 2024

Classification

  • Technology area (CPC H)Electricity
  • CPC primaryH10K71/12
  • WIPO fieldOrganic fine chemistry
  • WIPO sectorChemistry

Abstract

The present invention describes organic solvent-soluble Diels-Alder adducts of polycyclic aromatic compounds, such as, oligothiophene, perylene, benzo[ghi]perylene, coronene and polyacenes, with variety of dienophiles containing at least one heteroatom and in some cases two heteroatoms bonded to aromatic moiety, such as, thioxomalonates, azodicarboxylates, thialdehyde, acylnitroso and N-sulfinylamides. The Diels-Alder adducts are prepared by a simple, one step cycloaddition reaction of the polycyclic aromatic compounds, such as, pentacene, or other fused aromatic compounds, with heterodienophiles. The Diels-Alder adducts according to the present invention all form soluble adducts with pentacene and can be converted back to pentacene by retro-Diels-Alder reaction at moderate (60–250° C.) temperatures both in bulk, in solution or as thin-films.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.