Patent · US Expired

Method and apparatus for improved sensitivity in a mass spectrometer

US7256395B2 · kind B2 · utility

19Cited by
8References
20Claims
0Family size

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Inventors

Key dates

Filing dateJan 10, 2005
Grant dateAug 14, 2007
Priority date
Expiry dateJul 4, 2025

Classification

  • Technology area (CPC H)Electricity
  • CPC primaryH01J49/062
  • WIPO fieldElectrical machinery, apparatus, energy
  • WIPO sectorElectrical engineering

Abstract

In a mass spectrometer, ions from an ion source pass through an inlet aperture into a vacuum chamber for transmitting prior to mass analysis by the mass analyzer. The configuration of the inlet aperture forms a sonic orifice or sonic nozzle and with a predetermined vacuum chamber pressure, a supersonic free jet expansion is created in the vacuum chamber that entrains the ions within the barrel shock and Mach disc. Once formed, an ion guide with a predetermined cross-section to essentially radially confine the supersonic free jet expansion can focus the ions for transmission through the vacuum chamber. This effectively improves the ion transmission between the ion source and the mass analyzer.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.