Patent · US Expired

Microwave assisted chemical synthesis instrument with controlled pressure release

US7282184B2 · kind B2 · utility

9Cited by
31References
6Claims
0Family size

Assignee

Inventors

Key dates

Filing dateApr 19, 2002
Grant dateOct 16, 2007
Priority date
Expiry dateJun 21, 2024

Classification

  • Technology area (CPC Y)Emerging Cross-Sectional Technologies
  • CPC primaryY10T436/25
  • WIPO fieldElectrical machinery, apparatus, energy
  • WIPO sectorElectrical engineering

Abstract

An instrument is disclosed for carrying out controlled microwave assisted chemical processes, and that is particularly useful for handling relatively small samples. The instrument includes a microwave-transparent reaction vessel with an open mouth, a pressure-resistant seal on the mouth of the vessel, and a needle, portions of which penetrate the seal with a first end of the needle and provide fluid communication into the vessel. A pressure transducer is at the opposite end of the needle and in fluid communication with the interior of the vessel through the needle. The instrument defines a pressure control flow path from a portion of the needle outside of the vessel to a fluid port, the flow path being in communication with the needle, the interior of the vessel and the transducer. A controllable pressure release valve for the flow path is-associated with the port.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.