Patent · US Expired

Method of modifying zeolite catalyst

US7285511B2 · kind B2 · utility

21Cited by
176References
23Claims
0Family size

Assignee

Inventors

Key dates

Filing dateApr 23, 2004
Grant dateOct 23, 2007
Priority date
Expiry dateApr 21, 2025

Classification

  • Technology area (CPC Y)Emerging Cross-Sectional Technologies
  • CPC primaryY02P20/52
  • WIPO fieldOrganic fine chemistry
  • WIPO sectorChemistry

Abstract

A method of modifying a zeolite catalyst to increase para-xylene selectivity of the zeolite catalyst in toluene methylation reactions is provided. The method includes forming a slurry of a ZSM-5-type zeolite and an aqueous solution of a phosphorus compound. Water is removed from the slurry to provide a non-steamed, phosphorus treated ZSM-5 zeolite catalyst without deposition of phosphorus onto the catalyst by organophosphorus vapor deposition. The resulting non-steamed, phosphorus treated ZSM-5 zeolite catalyst has a pore volume of from 0.2 ml/g or less and provides greater than 80% para-xylene selectivity of mixed xylenes when used in toluene methylation.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.