Patent · US Expired

Real time methylumbelliferone-based assay

US7488721B2 · kind B2 · utility

4Cited by
1References
3Claims
0Family size

Assignees

Inventors

Key dates

Filing dateMay 13, 2005
Grant dateFeb 10, 2009
Priority date
Expiry dateMay 13, 2025

Classification

  • Technology area (CPC G)Physics
  • CPC primaryG01N2500/00
  • WIPO fieldBiotechnology
  • WIPO sectorChemistry

Abstract

A method is provided for determining the activity of an enzyme which releases methylumbelliferone (MU) from an MU-containing substrate wherein the enzyme has a pH optimum below the pKa of MU comprising: contacting a sample suspected of containing the enzyme with the MU-containing substrate at a pH suitable for activity of the enzyme to allow release of MU by the enzyme; contacting the sample with light of a wavelength in the range of about 310 nm to about 350 nm; determining fluorescence produced by the released MU, thereby determining the activity of the enzyme. This real time method provides improved diagnostic methods, for example for diseases associated with an abnormal level of activity of a glycosidase. The real time assay also can be used to screen compounds for their ability to modulate enzyme activity using MU-containing substrates.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.