Process for making solid triphenylboron-pyridine or its adduct
US7517985B2 · kind B2 · utility
2Cited by
1References
4Claims
0Family size
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Key dates
| Filing date | Jun 23, 2006 |
| Grant date | Apr 14, 2009 |
| Priority date | — |
| Expiry date | May 30, 2027 |
Classification
- Technology area (CPC C)Chemistry; Metallurgy
- CPC primaryC07F5/027
- WIPO fieldOrganic fine chemistry
- WIPO sectorChemistry
Abstract
A process for producing solid triphenylboron-pyridine (TPBP) spherical particles by separately feeding into a vigorously agitated reaction zone (i) a stream of pyridine and a (ii) stream comprising a solution of sodium hydroxide adduct of triphenylboron (TPBA) whereby the total concentration of TPBA in the combined feed streams is in the range of from 1 wt % to 6 wt %, and simultaneously removing a product stream from said reaction zone and recovering the triphenylboron-pyridine (TPBP) particles.
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