Patent · US Expired

Process for reactive esterification distillation

US7667068B2 · kind B2 · utility

43Cited by
12References
21Claims
0Family size

Assignee

Inventors

Key dates

Filing dateApr 28, 2006
Grant dateFeb 23, 2010
Priority date
Expiry dateApr 28, 2026

Classification

  • Technology area (CPC Y)Emerging Cross-Sectional Technologies
  • CPC primaryY02P20/10
  • WIPO fieldChemical engineering
  • WIPO sectorChemistry

Abstract

A process for producing organic acid di- or tri-esters, particularly citric acid tri-esters, with the available acid groups esterified using countercurrent reactive distillation using acid catalysts in a structured packing is described. In the reactive distillation an organic acid di- or tri-ester is formed by chemical reaction and purified to its final state within the single column. Organic acid di- or tri-esters are produced at relatively low cost, with less waste production in by-products of the reaction, and in a less complicated manner than prior processes. Organic acid di- and tri-esters have uses as solvents, as plasticizers and in conversion products.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.