Patent · US Expired

Metal passivation in a heat exchange reformer

US7727509B2 · kind B2 · utility

12Cited by
9References
11Claims
0Family size

Assignee

Inventors

Key dates

Filing dateDec 16, 2002
Grant dateJun 1, 2010
Priority date
Expiry dateDec 11, 2025

Classification

  • Technology area (CPC Y)Emerging Cross-Sectional Technologies
  • CPC primaryY02P20/10
  • WIPO fieldChemical engineering
  • WIPO sectorChemistry

Abstract

A method for reducing the interaction between carbon monoxide present in a heat exchange medium and metals on the shell side of heat exchange reformer apparatus used for reforming of hydrocarbons by treatment of the shell-side of said apparatus with an effective amount of at least one passivation compound containing at least one element selected from phosphorus, tin, antimony, arsenic, lead, bismuth, copper, germanium, silver or gold is described. Where volatile compounds are formed by the passivation compound, the method further comprises compound recovery to prevent contamination and deactivation of subsequent process steps. The method reduces side reactions, provides improved reformer tube lifetime and allows tubes to be treated in-situ without the need for process shutdown.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.