Patent · US Active

Preparation of acetic acid

US8076512B2 · kind B2 · utility

3Cited by
9References
15Claims
0Family size

Assignees

Inventors

Key dates

Filing dateAug 27, 2009
Grant dateDec 13, 2011
Priority date
Expiry dateMar 18, 2030

Classification

  • Technology area (CPC C)Chemistry; Metallurgy
  • CPC primaryC07C51/44
  • WIPO fieldOrganic fine chemistry
  • WIPO sectorChemistry

Abstract

A method for reducing aldehydes in an acetic acid production process is disclosed. The acetic acid is produced by reacting methanol and carbon monoxide in the presence of a carbonylation catalyst. The method comprises reacting an aldehyde-containing stream with an alcohol to form an acetal-containing stream. An acetal-enriched stream is separated from the acetal-containing stream and then hydrolyzed to form a hydrolysis mixture comprising the alcohol and the aldehydes. The alcohol is isolated from the hydrolysis mixture and used to react with the aldehyde-containing stream to form the acetal-containing stream. The invention reduces aldehydes in the acetic acid produced.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.