Method for the preparation of high purity stannous oxide
US8277774B2 · kind B2 · utility
Assignee
Inventors
Key dates
| Filing date | Jan 26, 2012 |
| Grant date | Oct 2, 2012 |
| Priority date | — |
| Expiry date | Jan 26, 2032 |
Classification
- Technology area (CPC C)Chemistry; Metallurgy
- CPC primaryC01P2006/80
- WIPO fieldMaterials, metallurgy
- WIPO sectorChemistry
Abstract
Provided herein are methods for the preparation of high purity stannous oxide comprising: (a) reacting a Sn salt with a C2-12 dicarboxylic acid in the aqueous phase to form a suspension comprising a Sn-dicarboxylate complex; (b) washing the Sn-dicarboxylate complex with water to obtain a wash solution comprising a washed Sn-dicarboxylate complex essentially free of the anion of the Sn salt; and (c) reacting the washed Sn-dicarboxylate complex with a base to form high purity SnO, wherein the high purity SnO has an alpha radiation count of less than about 0.002 cph/cm2.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.