Patent · US Active

Electrospray ionization mass spectrometry methodology

US8530834B2 · kind B2 · utility

3Cited by
9References
20Claims
0Family size

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Inventors

Key dates

Filing dateFeb 6, 2012
Grant dateSep 10, 2013
Priority date
Expiry dateFeb 6, 2032

Classification

  • Technology area (CPC G)Physics
  • CPC primaryG01N33/28
  • WIPO fieldMeasurement
  • WIPO sectorInstruments

Abstract

A method of enhanced speciation of both positive and negatives species in an analyte is disclosed. The method can include producing a first analyte solution comprising an analyte composition and an effective amount of silver triflate, and analyzing the first analyte solution with an electrospray ionization mass spectrometer. The method can also include producing a second analyte solution comprising a portion of the analyte composition and an effective amount of a compound of formula I, and analyzing the second analyte solution with an electrospray ionization mass spectrometer. The compound of formula I is [NX+][OH−], where X is a linear, branched, or cyclic C1-C10 alkane; an aryl; a heterocyclic aromatic; or a heterocyclic moiety.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.