Method for preparing main hydrolysate by hydrolyzing plant cellulose materials with concentrated sulfuric acid
US8603251B2 · kind B2 · utility
Inventor
Key dates
| Filing date | Jul 29, 2008 |
| Grant date | Dec 10, 2013 |
| Priority date | — |
| Expiry date | Mar 18, 2030 |
Classification
- Technology area (CPC Y)Emerging Cross-Sectional Technologies
- CPC primaryY02E50/10
- WIPO fieldOrganic fine chemistry
- WIPO sectorChemistry
Abstract
The present invention relates to a method to dispose plant cellulose materials, in particular to a method for preparing a main hydrolysate by hydrolyzing the plant cellulose materials with concentrated sulfuric acid. The plant cellulose materials are mixed with sulfuric acid in batches, and the main hydrolysate is obtained after hydrolysis. The batch mixing includes the following procedures: (1) sulfuric acid solution is used to dissolve part of the plant cellulose materials thereby forming a hydrolysate; (2) when the plant cellulose materials can not be dissolved any more, concentrated sulfuric acid with the concentration more than 80 wt % is successively added into the hydrolysate, and another part of the plant cellulose materials are added; (3) and then the procedure as step (2) is repeated until all the plant cellulose materials are completely hydrolyzed. The method utilizing concentrated sulfuric acid to prepare the main hydrolysate can hydrolyze the maximum cellulose with the least sulfuric acid, thereby decreasing the acid recovery cost proportioned by per kilogram sugar obtained by hydrolysis.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.