Method of operating a distillation column for purifying 1,2-dichloroethane and for coupled sodium hydroxide solution evaporative concentration
US8742182B2 · kind B2 · utility
Assignees
Inventors
Key dates
| Filing date | Sep 7, 2006 |
| Grant date | Jun 3, 2014 |
| Priority date | — |
| Expiry date | Oct 30, 2030 |
Classification
- Technology area (CPC C)Chemistry; Metallurgy
- CPC primaryC07C17/383
- WIPO fieldOrganic fine chemistry
- WIPO sectorChemistry
Abstract
Process for operating a distillation column for the removal of water and lower-boiling components than 1,2-dichloroethane from 1,2-dichloroethane in which at least part of the heat from condensation of the aqueous vapors from the distillation column is used to concentrate caustic soda solution by evaporation; furthermore, at least part of the 1,2-dichloroethane formed when chlorine and ethylene react in a direct chlorination unit is used to heat said distillation column and can subsequently also be used as a heat transfer fluid to concentrate caustic soda solution by evaporation.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.