Patent · US Active

Method of operating a distillation column for purifying 1,2-dichloroethane and for coupled sodium hydroxide solution evaporative concentration

US8742182B2 · kind B2 · utility

1Cited by
2References
3Claims
0Family size

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Key dates

Filing dateSep 7, 2006
Grant dateJun 3, 2014
Priority date
Expiry dateOct 30, 2030

Classification

  • Technology area (CPC C)Chemistry; Metallurgy
  • CPC primaryC07C17/383
  • WIPO fieldOrganic fine chemistry
  • WIPO sectorChemistry

Abstract

Process for operating a distillation column for the removal of water and lower-boiling components than 1,2-dichloroethane from 1,2-dichloroethane in which at least part of the heat from condensation of the aqueous vapors from the distillation column is used to concentrate caustic soda solution by evaporation; furthermore, at least part of the 1,2-dichloroethane formed when chlorine and ethylene react in a direct chlorination unit is used to heat said distillation column and can subsequently also be used as a heat transfer fluid to concentrate caustic soda solution by evaporation.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.