Method of preparing crystalline titanium dioxide powder, method of preparing a negative active material, negative active material, and rechargebale lithium battery
US8926938B2 · kind B2 · utility
Assignee
Inventors
Key dates
| Filing date | Jan 13, 2010 |
| Grant date | Jan 6, 2015 |
| Priority date | — |
| Expiry date | Feb 22, 2032 |
Classification
- Technology area (CPC Y)Emerging Cross-Sectional Technologies
- CPC primaryY02E60/10
- WIPO fieldElectrical machinery, apparatus, energy
- WIPO sectorElectrical engineering
Abstract
A method of manufacturing crystalline titanium dioxide (TiO2) powder, a method of a negative active material, and a negative active material and a rechargeable lithium battery including the crystalline titanium dioxide (TiO2) powder are provided. The method of manufacturing the crystalline titanium dioxide powder may include: preparing a titanyl chloride (TiOCl2) aqueous solution by adding titanium tetrachloride (TiCl4) to water at a temperature ranging from 0° C. to 10° C.; adding alcohol, urea, and a sphere-shaping agent to the titanyl chloride aqueous solution to prepare a mixture; and hydrothermally synthesizing the mixture under a pressure ranging from 1.5 atm to 5 atm at a temperature ranging from 80° C. to 155° C.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.