Liquid crystal polyester fibers and method for producing the same
US9011743B2 · kind B2 · utility
Assignee
Inventors
Key dates
| Filing date | Mar 4, 2010 |
| Grant date | Apr 21, 2015 |
| Priority date | — |
| Expiry date | Apr 30, 2031 |
Classification
- Technology area (CPC Y)Emerging Cross-Sectional Technologies
- CPC primaryY10T442/183
- WIPO fieldTextile and paper machines
- WIPO sectorMechanical engineering
Abstract
Disclosed are liquid crystal polyester fibers, which have a peak half-width of 15° C. or greater at an endothermic peak (Tm1) observed by differential calorimetry under a temperature elevation of 20° C./minute from 50° C., polystyrene equivalent weight average molecular weight of 250,000 or more and 2,000,000 or less, and a variable waveform of less than 10% in terms of the half inert diagram mass waveform determined by a Uster yarn irregularity tester. Also disclosed is a method for producing liquid crystal polyester fibers, wherein liquid crystal polyester fibers are formed into a package, the fibers are then subjected to solid-phase polymerization, and the solid-phase polymerized liquid crystal polyester fibers are unrolled from the package and successively heat treated without being once taken up. The heat treatment temperature is controlled at a temperature of the endothermic peak temperature (Tm1) of the solid-phase polymerized liquid crystal polyester fibers+60° C. or higher, and the speeds of the fibers before and after heat treatment are regulated, respectively, by first and second rollers.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.