Patent · US Active

Polycarbonate preparation method

US9062154B2 · kind B2 · utility

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6References
14Claims
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Key dates

Filing dateNov 5, 2012
Grant dateJun 23, 2015
Priority date
Expiry dateNov 5, 2032

Classification

  • Technology area (CPC C)Chemistry; Metallurgy
  • CPC primaryC08G64/406
  • WIPO fieldMacromolecular chemistry, polymers
  • WIPO sectorChemistry

Abstract

Provided is a polycarbonate preparation method, comprising the following steps: a) mixing a phenoxide water aqueous solution of a bisphenol and/or a polyphenol with a phosgene and an inert organic solvent, reacting, and generating a polycarbonate oligomer; b) highly emulsifying the oligomer by reinforced micromixing to form a stable emulsion; and c) introducing the emulsion into a polycondensation reactor for a chain extending reaction, separating and finally obtaining the polycarbonate. Through the reinforced micromixing, the present method can prepare the high-molecular-weight polycarbonate without any catalysts, thus simplifying the post-treatment process of the product and improving product quality.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.