Method for synthesizing rare earth metal extractant
US9133100B2 · kind B2 · utility
Assignees
Inventors
Key dates
| Filing date | Jul 1, 2011 |
| Grant date | Sep 15, 2015 |
| Priority date | — |
| Expiry date | Jul 1, 2031 |
Classification
- Technology area (CPC Y)Emerging Cross-Sectional Technologies
- CPC primaryY02W30/50
- WIPO fieldMaterials, metallurgy
- WIPO sectorChemistry
Abstract
A rare earth metal extractant containing, as the extractant component, dialkyldiglycol amide acid which is excellent in breaking down light rare earth elements is reacted in diglycolic acid (X mol) and an esterification agent (Y mol) at a reaction temperature of 70° C. or more and for a reaction time of one hour or more such that the mol ratio of Y/X is 2.5 or more, and is subjected to vacuum concentration. Subsequently, a reaction intermediate product is obtained by removing unreacted products and reaction residue. Then a nonpolar or low-polar solvent which is an organic solvent for forming an organic phase during solvent extraction of the rare earth metal and which is capable of dissolving dialkyldiglycol amide acid is added as the reaction solvent, and the reaction intermediate product is reacted with dialkyl amine (Z mol) such that the mol ratio of Z/X is 0.9 or more.
Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.