Patent · US Active

Method for the production of multiphase composite materials using microwave plasma process

US9242224B2 · kind B2 · utility

30Cited by
12References
18Claims
0Family size

Assignee

Inventors

Key dates

Filing dateMar 13, 2014
Grant dateJan 26, 2016
Priority date
Expiry dateMar 13, 2034

Classification

  • Technology area (CPC C)Chemistry; Metallurgy
  • CPC primaryC04B2235/764
  • WIPO fieldMaterials, metallurgy
  • WIPO sectorChemistry

Abstract

Disclosed herein is a method to produce multiphase composite materials directly from solution precursor droplets by a fast pyrolysis process using a microwave plasma embodiment containing a microwave generating source, a dielectric plasma torch, and a droplet maker. Here, using homogenous solution precursors, droplets are generated with a narrow size distribution, and are injected and introduced into the microwave plasma torch with generally uniform thermal path. The generally uniform thermal path in the torch is achieved by axial injection of droplets into an axisymmetric hot zone with laminar flows. Upon exposing to high temperature within the plasma with controlled residence time, the droplets are pyrolyzed and converted into particles by quenching with a controlled rate of the exhaust gas in a gas chamber. The particles generated have generally uniform sizes and uniform thermal history, and can be used for a variety of applications.

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.