Patent · US Active

Molecular glass of spirofluorene derivative, preparation method thereof and use thereof in photo-etching

US9290435B2 · kind B2 · utility

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19Claims
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Assignee

Inventors

Key dates

Filing dateJan 22, 2013
Grant dateMar 22, 2016
Priority date
Expiry dateJan 22, 2033

Classification

  • Technology area (CPC C)Chemistry; Metallurgy
  • CPC primaryC07C2603/94
  • WIPO fieldOrganic fine chemistry
  • WIPO sectorChemistry

Abstract

Disclosed is a molecular glass of a spirofluorene derivative having a molecular structure as follows: formula (I),wherein each of R1-R12 is a hydrogen atom, a hydroxyl group, a methoxyl group or an acid-sensitive substituent; substituents R1˜R12 can be identical or different, but on the same benzene ring the substituents cannot all be hydrogen atoms. The molecular glass has a good solubility in various polar solvents, is suitable to be made into a film; meanwhile the molecular glass has a very high glass transition temperature and meets the requirements of the photolithography processing technology. Also disclosed is a preparation method of the above-mentioned molecular glass of a spirofluorene derivative. The synthetic process of the method is simple and suitable for industrialization. Further disclosed is the use of a photo-resist with the above-mentioned molecular glass as a main material in photo-etching, wherein the molecular glass of a spirofluorene derivative with hydroxyl groups (or partly with hydroxyl groups) on the periphery thereof can be used as a negative photo-resist, and the molecular glass with the hydroxyl groups on the periphery thereof protected (or partly prote…

Source: USPTO / EPO open patent data. Objective bibliographic and citation counts.